(Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

Base Information

Chemical Name:(Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide
CAS No.:816425-69-1
Molecular Formula:C₁₁H₁₅NOS
Molecular Weight:209.312
Hs Code.:

Synonyms:(Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

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Chemical Property of (Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

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Technology Process of (Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

There total 2 articles about (Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Dimethyl-{2-[((Z)-propenyl)sulfanyl]-phenyl}-amine

: 816425-69-1
(Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

: 816425-70-4
(E)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1002/chem.200400443

Reference yield:

: 18206-22-9
bis[2-(N,N-dimethylamino)phenyl] disulfide

: 816425-69-1
(Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuLi / pentane; tetrahydrofuran / 2 h / -78 °C

1.2: tetrahydrofuran; pentane / 1 h / 0 °C

2.1: 318 mg / MCPBA / CH₂Cl₂ / 1 h / -78 °C

With tert.-butyl lithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; pentane;
DOI:10.1002/chem.200400443

Reference yield: 22.0%

: 816425-69-1
(Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide

: 693-02-7
hex-1-yne

: 2-n-butyl-5-[2-(N,N-dimethylamino)phenylsufinyl]-4-methyl-2-cyclopentenone

: 2-n-butyl-5-[2-(N,N-dimethylamino)phenylsulfinyl]-4-methyl-2-cyclopentenone

Guidance literature:: hex-1-yne; [Co₂(CO)8]; In acetonitrile; at 20 ℃; for 1h;

(Z)-2-(N,N-dimethylamino)phenyl 1-propenyl sulfoxide; With 4-methylmorpholine N-oxide; In acetonitrile; at 20 ℃; for 48h; under 7500600 Torr;
DOI:10.1002/chem.200400443