N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

Base Information

Chemical Name:N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide
CAS No.:337919-23-0
Molecular Formula:C₂₅H₃₅NO₃Si
Molecular Weight:425.643
Hs Code.:

<i>N</i>-[8-(<i>tert</i>-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

Synonyms:N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

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Technology Process of N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

There total 3 articles about N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 337919-17-2
N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,8-dihydro-naphthalen-1-yl]-benzamide

: 337919-23-0
N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 760 Torr;
DOI:10.1055/s-2001-11408

Reference yield:

: 74213-12-0
(E)-5-<(tert-butyldimethylsilyl)oxy>-1,3-pentadiene

: 337919-23-0
N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 168 h / 9750780 Torr

2: 0.360 g / aq. HCl / tetrahydrofuran / 0.08 h / 20 °C

3: 97 percent / H₂ / Pd/C / tetrahydrofuran / 760 Torr

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; 1: Diels-Alder reaction;
DOI:10.1055/s-2001-11408

Reference yield:

: N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4,4-dimethoxy-4a,5,8,8a-tetrahydro-4H-naphthalen-1-ylidene]-benzamide

: 337919-23-0
N-[8-(tert-butyl-dimethyl-silanyloxymethyl)-4-methoxy-5,6,7,8-tetrahydro-naphthalen-1-yl]-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 0.360 g / aq. HCl / tetrahydrofuran / 0.08 h / 20 °C

2: 97 percent / H₂ / Pd/C / tetrahydrofuran / 760 Torr

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1055/s-2001-11408