Technology Process of C51H81NO15S
There total 7 articles about C51H81NO15S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C52H84NO15S(1+)*I(1-);
With
silver(I) chloride;
In
methanol;
at 20 ℃;
for 4h;
With
pyridine-4-thiol; sodium hydride;
In
acetonitrile;
at 20 - 90 ℃;
for 19h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methanol / 30 h / 40 °C
2.1: dichloromethane / 5 h / 25 °C
3.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
3.2: 2 h / 0 - 10 °C
4.1: silver(I) chloride / methanol / 4 h / 20 °C
4.2: 19 h / 20 - 90 °C / Inert atmosphere
With
methanol; sodium hydride; silver(I) chloride;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide / acetone / 2.5 h / 20 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 5 °C / Inert atmosphere; Ice cooling
3.1: methanol / 30 h / 40 °C
4.1: dichloromethane / 5 h / 25 °C
5.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
5.2: 2 h / 0 - 10 °C
6.1: silver(I) chloride / methanol / 4 h / 20 °C
6.2: 19 h / 20 - 90 °C / Inert atmosphere
With
methanol; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; silver(I) chloride;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; mineral oil;