Technology Process of C22H22FN3O3
There total 3 articles about C22H22FN3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2011.03.013
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / ethanol; water / 2 h / 20 °C
1.2: pH 1
2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; potassium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.013
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium acetate; acetic acid / 1.75 h / 35 - 90 °C
2.1: potassium hydroxide / ethanol; water / 2 h / 20 °C
2.2: pH 1
3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
With
sodium acetate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; potassium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.013
