phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate

Base Information

Chemical Name:phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate
CAS No.:1003945-22-9
Molecular Formula:C₂₅H₂₉N₃O₅
Molecular Weight:451.522
Hs Code.:

Synonyms:phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate

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Chemical Property of phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate

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Technology Process of phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate

There total 5 articles about phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 917833-89-7
2-(7-methoxy-2-oxoquinolin-1(2H)-yl)acetaldehyde

: 872716-81-9
phenylmethyl {[(3R,4S)-4-hydroxy-3-pyrrolidinyl]methyl}carbamate

: 1003945-22-9
phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate

Guidance literature:: 2-(7-methoxy-2-oxoquinolin-1(2H)-yl)acetaldehyde; phenylmethyl {[(3R,4S)-4-hydroxy-3-pyrrolidinyl]methyl}carbamate; With sodium carbonate; In methanol; dichloromethane; for 1h;

With sodium tris(acetoxy)borohydride; In methanol; dichloromethane;

Reference yield:

: 1003944-22-6
7-(methyloxy)-1-(2-propen-1-yl)quinolinium iodide

: 1003945-22-9
phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; water; potassium hexacyanoferrate(III) / 1,4-dioxane / 1.5 h / 20 °C

2: ozone / dichloromethane / 0.67 h / -78 °C

3: sodium carbonate / methanol; dichloromethane / 1 h

With potassium hydroxide; water; sodium carbonate; ozone; potassium hexacyanoferrate(III); In 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 4964-76-5
7-methoxyquinoline

: 1003945-22-9
phenylmethyl [((3S,4S)-4-hydroxy-1-{2-[7-(methyloxy)-2-oxo-1(2H)-quinolinyl]ethyl}-3-pyrrolidinyl)methyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 2.5 h / 95 - 120 °C

2: potassium hydroxide; water; potassium hexacyanoferrate(III) / 1,4-dioxane / 1.5 h / 20 °C

3: ozone / dichloromethane / 0.67 h / -78 °C

4: sodium carbonate / methanol; dichloromethane / 1 h

With potassium hydroxide; water; sodium carbonate; ozone; potassium hexacyanoferrate(III); In 1,4-dioxane; methanol; dichloromethane; toluene;