4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene

Base Information

Chemical Name:4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene
CAS No.:1338470-40-8
Molecular Formula:C₁₈H₁₈N₄S₂
Molecular Weight:354.5
Hs Code.:

Synonyms:4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene

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Chemical Property of 4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene

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Technology Process of 4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene

There total 3 articles about 4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1338470-32-8
4-methyl-2-phenyl-6H-1-thia-3,4-diazin-5-thione

: 90145-13-4
N-(α-Bromobenzylidene)-N'-methylhydrazine hydrobromide

: 1338470-40-8
4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; Reflux;
DOI:10.1080/10426507.2010.546587

Reference yield:

: 857749-37-2
4-methyl-2-phenyl-6H-1-thia-3,4-diazin-5-one

: 1338470-40-8
4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; tetraphosphorus decasulfide / 5,5-dimethyl-1,3-cyclohexadiene / 20 °C / Reflux

2: triethylamine / chloroform / 20 °C / Reflux

With pyridine; tetraphosphorus decasulfide; triethylamine; In 5,5-dimethyl-1,3-cyclohexadiene; chloroform;
DOI:10.1080/10426507.2010.546587

Reference yield:

: 90145-13-4
N-(α-Bromobenzylidene)-N'-methylhydrazine hydrobromide

: 1338470-40-8
4,6-dimethyl-2,8-diphenyl-1,9-dithia-3,4,6,7-tetraazaspiro[4.5]dec-2,7-diene

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran; methanol / -5 - 20 °C

2: pyridine; tetraphosphorus decasulfide / 5,5-dimethyl-1,3-cyclohexadiene / 20 °C / Reflux

3: triethylamine / chloroform / 20 °C / Reflux

With pyridine; tetraphosphorus decasulfide; triethylamine; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; chloroform;
DOI:10.1080/10426507.2010.546587