O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride

Base Information

Chemical Name:O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride
CAS No.:120403-35-2
Molecular Formula:C₅₆H₅₉ClO₁₁
Molecular Weight:943.531
Hs Code.:

Synonyms:O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride

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Chemical Property of O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride

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Technology Process of O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride

There total 9 articles about O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 120403-33-0
phenyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

: 120403-35-2
O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride

Guidance literature:: With chlorine; In tetrachloromethane; for 0.0833333h;
DOI:10.1016/0008-6215(88)80008-9

Reference yield:

: 120403-26-1
phenyl 2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

: 120403-35-2
O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / silver perchlorate, 2,4,6-trimethylpyridine / diethyl ether / 0.5 h / -20 °C

2: chlorine / CDCl₃ / 0.25 h

With 2,4,6-trimethyl-pyridine; silver perchlorate; chlorine; In diethyl ether; chloroform-d1;
DOI:10.1016/0008-6215(88)80008-9

Reference yield:

: 100-44-7
benzyl chloride

: 120403-35-2
O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / potassium hydroxide / dimethylsulfoxide / 2 h / Ambient temperature

2: 61 percent / p-toluenesulfonic acid / 2 h / 55 - 60 °C

3: 32 percent / silver perchlorate, 2,4,6-trimethylpyridine / diethyl ether / 0.5 h / -20 °C

4: chlorine / CDCl₃ / 0.25 h

With 2,4,6-trimethyl-pyridine; potassium hydroxide; silver perchlorate; chlorine; toluene-4-sulfonic acid; In diethyl ether; chloroform-d1; dimethyl sulfoxide;
DOI:10.1016/0008-6215(88)80008-9