1,8-Diphenyl-9,10-anthraquinon

Base Information

• Chemical Name: 1,8-Diphenyl-9,10-anthraquinon
• CAS No.: 33522-27-9
• Molecular Formula: C₂₆H₁₆O₂
• Molecular Weight: 360.412

Synonyms:1,8-Diphenyl-9,10-anthraquinon

Chemical Property of 1,8-Diphenyl-9,10-anthraquinon

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Technology Process of 1,8-Diphenyl-9,10-anthraquinon

There total 15 articles about 1,8-Diphenyl-9,10-anthraquinon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,8-diphenyl anthracene (33522-35-9) → 1,8-Diphenyl-9,10-anthraquinon (33522-27-9)

Guidance literature:

With potassium dichromate; sulfuric acid; In water; acetic acid; chlorobenzene; for 48h; Heating;

DOI:10.1021/jo01298a013

Reference yield: 76.8%

1,8-dichloroanthraquinone (82-43-9) + phenylboronic acid (98-80-6) → 1,8-Diphenyl-9,10-anthraquinon (33522-27-9)

Guidance literature:

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; for 24h; Reflux;

Reference yield: 36.0%

C26H18O2 (73274-96-1) → 1,8-Diphenyl-9,10-anthraquinon (33522-27-9) + 10-Hydroxy-4,5-diphenyl-10H-anthracen-9-one (73274-98-3) + 1,8-Diphenyl-9,10-dihydro-anthracene-9,10-diol (73274-97-2)

Guidance literature:

With dimethylsulfide; In tetrahydrofuran; Heating;

DOI:10.1021/jo01298a013

upstream raw materials:

1,8-diphenyl anthracene

C₂₆H₁₈O₂

1,8-Diphenyl-1,4-dihydro-anthraquinone

1,8-diiodo-anthraquinone

Downstream raw materials:

1,8-Diphenyl-<9>anthron

10-Ethynyl-10-hydroxy-1,8-diphenyl-10H-anthracen-9-one

1,8-diphenyl anthracene

10-Hydroxy-1,8,10-triphenyl-10H-anthracen-9-one

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