β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)

Base Information

• Chemical Name: β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)
• CAS No.: 765274-02-0
• Molecular Formula: C₁₇H₂₂O₆
• Molecular Weight: 322.358

Synonyms:β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)

Chemical Property of β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)

There total 3 articles about β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,5-di-O-benzoyl-β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate) (765274-01-9) → β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate) (765274-02-0)

Guidance literature:

With methanol; sodium methylate; at 25 ℃; for 1h;

DOI:10.1039/c6sc04866h

Reference yield:

n-Pent-4-enyl alcohol (821-09-0) → β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate) (765274-02-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / 2,6-lutidine; tetra-n-butylammonium iodide / CH₂Cl₂ / 72 h / Heating

2: 75 percent / NaOMe / methanol; CH₂Cl₂ / 2 h / 20 °C

With 2,6-dimethylpyridine; sodium methylate; tetra-(n-butyl)ammonium iodide; In methanol; dichloromethane;

DOI:10.1021/ol0490680

Reference yield:

2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl bromide (4348-68-9) → β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate) (765274-02-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / 2,6-lutidine; tetra-n-butylammonium iodide / CH₂Cl₂ / 72 h / Heating

2: 75 percent / NaOMe / methanol; CH₂Cl₂ / 2 h / 20 °C

With 2,6-dimethylpyridine; sodium methylate; tetra-(n-butyl)ammonium iodide; In methanol; dichloromethane;

DOI:10.1021/ol0490680

upstream raw materials:

3,5-di-O-benzoyl-β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)

n-Pent-4-enyl alcohol

2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl bromide

Downstream raw materials:

3,5-di-O-benzyl-β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)

(3aS,5R,6R,6aS)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2-pent-4-enyloxy-2-phenyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-ol

4-pentenyl 3,5-di-O-benzyl-α-D-arabinofuranoside

pent-4-enyl 2-O-benzoyl-3-O-benzyl-α-D-arabinofuranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 765274-02-0 β-D-arabinofuranose 1,2-(pent-4-enyl orthobenzoate)

Send

Send

Metric Ton KG G Pound L ML

Send

Send