2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole

Base Information

Chemical Name:2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole
CAS No.:1355953-23-9
Molecular Formula:C₂₃H₂₅NO₄S₂
Molecular Weight:443.588
Hs Code.:

Synonyms:2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole

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Chemical Property of 2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole

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Technology Process of 2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole

There total 2 articles about 2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1355953-25-1
C₁₆H₂₁BrO₄

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 1355953-23-9
2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.carres.2011.11.005

Reference yield:

: 57575-19-6,81686-55-7
2-[(3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol

: 1355953-23-9
2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; triphenylphosphine / N,N-dimethyl-formamide / 50 °C

2: sodium hydride / tetrahydrofuran / 0 °C

With N-Bromosuccinimide; sodium hydride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.11.005

Reference yield: 75.0%

: 1355953-23-9
2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)thio)benzo[d]thiazole

: 1355953-27-3
2-((2-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethyl)sulfonyl)benzo[d]thiazole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 4h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2011.11.005