diethyl phosphorofluoridothioate

Base Information

• Chemical Name: diethyl phosphorofluoridothioate
• CAS No.: 358-75-8
• Molecular Formula: C₄H₁₀FO₂PS
• Molecular Weight: 172.16

Synonyms:diethyl phosphorofluoridothioate

Chemical Property of diethyl phosphorofluoridothioate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of diethyl phosphorofluoridothioate

There total 2 articles about diethyl phosphorofluoridothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Imidazol-1-yl-phosphonothioic acid O,O-diethyl ester (107313-21-3) → 1-benzoylimidazole (10364-94-0) + diethyl phosphorofluoridothioate (358-75-8)

Guidance literature:

With benzoyl fluoride; In dichloromethane; 1.) 0 deg C, 2.) 1 h, room temperature;

DOI:10.1016/S0040-4039(00)95535-7

Reference yield:

benzoyl fluoride (455-32-3) + Imidazol-1-yl-phosphonothioic acid O,O-diethyl ester (107313-21-3) → 1-benzoylimidazole (10364-94-0) + diethyl phosphorofluoridothioate (358-75-8)

Guidance literature:

In dichloromethane; 1.) 0 deg C, 2.) 1 h, room temperature;

DOI:10.1016/S0040-4039(00)95535-7

Reference yield:

diethyl phosphorofluoridothioate (358-75-8) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → Dimethylaethylaniliniumsalz der Monoaethylthiol-monofluoro-monophosphorsaeure (1652-54-6)

Guidance literature:

upstream raw materials:

benzoyl fluoride

Imidazol-1-yl-phosphonothioic acid O,O-diethyl ester

Downstream raw materials:

Dimethylaethylaniliniumsalz der Monoaethylthiol-monofluoro-monophosphorsaeure

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