N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide

Base Information

Chemical Name:N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide
CAS No.:188685-43-0
Molecular Formula:C₅₄H₅₄N₁₂O₉
Molecular Weight:1015.1
Hs Code.:

Synonyms:N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide

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Chemical Property of N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide

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Technology Process of N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide

There total 3 articles about N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 4422-95-1
1,3,5-benzene tris(carbonyl chloride)

: 188685-41-8
3'-tertiary-butoxycarbonylamino-2,2'-bipyridine-3-amine

: 188685-43-0
N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide

Guidance literature:: With TEA; In tetrahydrofuran; for 18h; Ambient temperature;
DOI:10.1002/chem.19970030220

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 188685-43-0
N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / tetrahydrofuran / 18 h / Heating

2: 83 percent / TEA / tetrahydrofuran / 18 h / Ambient temperature

With TEA; In tetrahydrofuran;
DOI:10.1002/chem.19970030220

Reference yield:

: 75449-26-2
2,2'-bipyridine-3,3'-diamine

: 188685-43-0
N,N',N-Tris[3(3'-t-butoxycarbonylamino-2,2'-bipyridyl)]benzene-1,3,5-tricarbonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / tetrahydrofuran / 18 h / Heating

2: 83 percent / TEA / tetrahydrofuran / 18 h / Ambient temperature

With TEA; In tetrahydrofuran;
DOI:10.1002/chem.19970030220