4-(4-bromo-benzyl)-[1,4']bipiperidinyl

Base Information

Chemical Name:4-(4-bromo-benzyl)-[1,4']bipiperidinyl
CAS No.:362512-04-7
Molecular Formula:C₁₇H₂₅BrN₂
Molecular Weight:337.303
Hs Code.:

Synonyms:4-(4-bromo-benzyl)-[1,4']bipiperidinyl

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Chemical Property of 4-(4-bromo-benzyl)-[1,4']bipiperidinyl

Chemical Property:

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Technology Process of 4-(4-bromo-benzyl)-[1,4']bipiperidinyl

There total 5 articles about 4-(4-bromo-benzyl)-[1,4']bipiperidinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 203187-19-3
4-(4-bromo-benzyl)-[1,4']bipiperidinyl-1'-carboxylic acid tert-butyl ester

: 362512-04-7
4-(4-bromo-benzyl)-[1,4']bipiperidinyl

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; dichloromethane; Heating;
DOI:10.1016/j.bmcl.2005.01.016

Reference yield:

: 31252-42-3
4-benzylpyperidine

: 362512-04-7
4-(4-bromo-benzyl)-[1,4']bipiperidinyl

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / CH₂Cl₂

2: 45 percent / 1,3-dibromo-5,5-dimethylhydantoin; CH₃SO₃H / CH₂Cl₂

3: 99 percent / aq. K₂CO₃ / methanol

4: 58 percent / NaB(OAc)3H; AcOH / 1,2-dichloro-ethane

5: 100 percent / HCl / dioxane; methanol; CH₂Cl₂ / Heating

With hydrogenchloride; methanesulfonic acid; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; In 1,4-dioxane; methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2005.01.016

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 362512-04-7
4-(4-bromo-benzyl)-[1,4']bipiperidinyl

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / NaB(OAc)3H; AcOH / 1,2-dichloro-ethane

2: 100 percent / HCl / dioxane; methanol; CH₂Cl₂ / Heating

With hydrogenchloride; sodium tris(acetoxy)borohydride; acetic acid; In 1,4-dioxane; methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2005.01.016