3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole

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Chemical Name:3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole
CAS No.:1416956-60-9
Molecular Formula:C₂₄H₁₇BrCl₂N₂O₄
Molecular Weight:548.22
Hs Code.:

Synonyms:3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole

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Chemical Property of 3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole

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Technology Process of 3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole

There total 11 articles about 3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416956-65-4
C₃₁H₂₃BrCl₂N₂O₆S

: 1416956-60-9
3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 1h;
DOI:10.1039/c2cc37110c

Reference yield:

: 1416956-54-1
methyl 3-bromo-4,5-dichloro-1-(3-methoxy-2-methylidene-3-oxo-propyl)-1H-pyrrole-2-carboxylate

: 1416956-60-9
3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 11 steps

1.1: ozone; oxygen / dichloromethane / 0.3 h / -78 °C

1.2: 6.5 h

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / -42 °C

2.2: -42 - 20 °C

3.1: toluene / 16 h / Reflux

4.1: ozone; oxygen / methanol; dichloromethane / 0.2 h / -78 °C

4.2: 14 h

5.1: ammonium acetate; acetic acid / 0.5 h

6.1: dmap; N-ethyl-N,N-diisopropylamine / 24 h / Cooling

7.1: diisobutylaluminium hydride / toluene; dichloromethane / 10.5 h / 0 °C

8.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 15 h / 70 °C

9.1: tetrahydrofuran / 4 h / 0 °C

10.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 29 h / 70 °C

10.2: 4 h / 0 °C

11.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h / 20 °C

With dmap; ammonium acetate; oxygen; sodium hydride; diisobutylaluminium hydride; ozone; acetic acid; N-ethyl-N,N-diisopropylamine; potassium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1039/c2cc37110c

Reference yield:

: 1416956-52-9
methyl 3-bromo-4,5-dichloro-1-(1-methoxy-1,2,5-trioxopentan-3-yl)-1H-pyrrole-2-carboxylate

: 1416956-60-9
3-bromo-4,5-dichloro-2-[(2-methoxyphenyl)carbonyl]-1-(2-[(2-methoxyphenyl)carbonyl]-1H-pyrrol-3-yl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonium acetate; acetic acid / 0.5 h

2.1: dmap; N-ethyl-N,N-diisopropylamine / 24 h / Cooling

3.1: diisobutylaluminium hydride / toluene; dichloromethane / 10.5 h / 0 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 15 h / 70 °C

5.1: tetrahydrofuran / 4 h / 0 °C

6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 29 h / 70 °C

6.2: 4 h / 0 °C

7.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h / 20 °C

With dmap; ammonium acetate; diisobutylaluminium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; potassium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1039/c2cc37110c