C₁₃H₁₅N₅O

Base Information

Chemical Name:C₁₃H₁₅N₅O
CAS No.:1209487-51-3
Molecular Formula:C₁₃H₁₅N₅O
Molecular Weight:257.295
Hs Code.:

C<sub>13</sub>H<sub>15</sub>N<sub>5</sub>O

Synonyms:C₁₃H₁₅N₅O

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Chemical Property of C₁₃H₁₅N₅O

Chemical Property:

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Technology Process of C₁₃H₁₅N₅O

There total 11 articles about C₁₃H₁₅N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 108-86-1,52753-63-6
bromobenzene

: 1209492-67-0
C₇H₁₁N₅O

: 1209487-51-3
C₁₃H₁₅N₅O

Guidance literature:: With caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 100 ℃; for 7h; Inert atmosphere;

Reference yield:

: 1200497-52-4
3,5-dimethyl 1-[2-(benzyloxy)ethyl]-1H-pyrazole-3,5-dicarboxylate

: 1209487-51-3
C₁₃H₁₅N₅O

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium hydroxide; methanol / 20 °C / Inert atmosphere

2.1: triethylamine; diphenyl phosphoryl azide / 4 h / 100 °C / Inert atmosphere

3.1: hydrogen / 20% palladium(II) hydroxide on carbon / water; methanol / 6 h / 20 °C

4.1: tributylphosphine; 1,1'-(Azodicarbonyl)dipiperidin / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere

5.1: water; lithium hydroxide / tetrahydrofuran; methanol / 1.5 h / 20 °C

6.1: triethylamine; diphenyl phosphoryl azide / toluene / 5.5 h / 100 °C / Inert atmosphere

7.1: hydrogen / 20% palladium(II) hydroxide on carbon / water; tetrahydrofuran; methanol / 20 °C

8.1: pyridine / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

8.2: 1 h / 0 - 20 °C / Inert atmosphere

9.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 5.5 h / 20 °C

10.1: triethylamine / chloroform / 0.5 h / 0 - 20 °C

11.1: caesium carbonate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 7 h / 100 °C / Inert atmosphere

With pyridine; hydrogenchloride; methanol; tributylphosphine; diphenyl phosphoryl azide; 1,1'-(Azodicarbonyl)dipiperidin; water; hydrogen; caesium carbonate; triethylamine; potassium hydroxide; lithium hydroxide; 20% palladium(II) hydroxide on carbon; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; toluene;

Reference yield:

: 1200497-67-1
C₁₂H₁₇N₃O₄

: 1209487-51-3
C₁₃H₁₅N₅O

Guidance literature:: Multi-step reaction with 7 steps

1.1: water; lithium hydroxide / tetrahydrofuran; methanol / 1.5 h / 20 °C

2.1: triethylamine; diphenyl phosphoryl azide / toluene / 5.5 h / 100 °C / Inert atmosphere

3.1: hydrogen / 20% palladium(II) hydroxide on carbon / water; tetrahydrofuran; methanol / 20 °C

4.1: pyridine / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

4.2: 1 h / 0 - 20 °C / Inert atmosphere

5.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 5.5 h / 20 °C

6.1: triethylamine / chloroform / 0.5 h / 0 - 20 °C

7.1: caesium carbonate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 7 h / 100 °C / Inert atmosphere

With pyridine; hydrogenchloride; diphenyl phosphoryl azide; water; hydrogen; caesium carbonate; triethylamine; lithium hydroxide; 20% palladium(II) hydroxide on carbon; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; toluene;