(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide

Base Information

Chemical Name:(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide
CAS No.:960060-71-3
Molecular Formula:C₃₂H₄₆F₃NO₄Si
Molecular Weight:593.802
Hs Code.:

Synonyms:(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide

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Chemical Property of (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide

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Technology Process of (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide

There total 2 articles about (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 960060-57-5
C₃₂H₄₆F₃NO₄Si

: 960060-71-3
(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide

Guidance literature:: With di-μ-chlorobis[η⁵-(S)-(S_p)-2-(2'-(4'-methylethyl)oxazolinyl)cyclopentadienyl, (1-C,3'-N)(η⁵-pentaphenylcyclopentadiene)ferrocene]dipalladium; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; silver nitrate; In dichloromethane; at 50 ℃; for 48h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900712

Reference yield: 51.0%

: (Z)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-(3-triisopropyloxysilylpropyl)-5-benzyloxypent-2-enyl ester

: 960060-71-3
(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(1-benzyloxymethyl-1-[3-triisopropylsilyloxypropyl]allyl)acetamide

Guidance literature:: With silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; ferrocenyl 1-Ts-2,3-Ph₂-imidazoline palladacycle catalyst; In dichloromethane; at 50 ℃; for 84h;
DOI:10.1002/anie.200702086