(S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride

Base Information

Chemical Name:(S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride
CAS No.:1350520-00-1
Molecular Formula:C₂₁H₂₇N₃O₂*ClH
Molecular Weight:389.925
Hs Code.:

Synonyms:(S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride

Chemical Property:

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Technology Process of (S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride

There total 3 articles about (S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350519-99-1
C₂₆H₃₅N₃O₄

: 1350520-00-1
(S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.09.079

Reference yield:

: 100-46-9
benzylamine

: 1350520-00-1
(S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0.08 h / Inert atmosphere

1.2: 20 h / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.079

Reference yield:

: 108334-64-1
N-tert-butyloxycarbonyl-L-valyl-L-phenylalanine

: 1350520-00-1
(S)-2-amino-N-(1-(benzylamino)-1-oxo-3-phenylpropan-2-yl)-3-methylbutanamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0.08 h / Inert atmosphere

1.2: 20 h / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.079