(S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester

Base Information

• Chemical Name: (S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester
• CAS No.: 887130-21-4
• Molecular Formula: C₂₁H₃₄O₄Si
• Molecular Weight: 378.584

Synonyms:(S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester

Chemical Property of (S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester

There total 2 articles about (S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-(R)-2-{(S)-Acetoxy-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-methyl}-2-methyl-pent-3-enoic acid methyl ester → (S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester (887130-21-4)

Guidance literature:

With hydrazine; In methanol; at 0 ℃; for 3h;

DOI:10.1021/ja061082f

Reference yield:

2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester + acetic anhydride (108-24-7) → (R,S)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester (887130-20-3) + (S,R)-2-{[2-(tert-butyldimethylsilanyloxymethyl)-phenyl]-hydroxymethyl}-2-methylpent-3-enoic acid methyl ester (887130-21-4) + (E)-(S)-2-{(R)-Acetoxy-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-methyl}-2-methyl-pent-3-enoic acid methyl ester + (E)-(R)-2-{(S)-Acetoxy-[2-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-methyl}-2-methyl-pent-3-enoic acid methyl ester

Guidance literature:

With (S)-(-)-C₅Ph₅-DMAP(Fe); triethylamine; In tert-Amyl alcohol; at 0 ℃; for 114h; Title compound not separated from byproducts;

DOI:10.1021/ja061082f

upstream raw materials:

acetic anhydride

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