allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:1603826-96-5
Molecular Formula:C₄₄H₅₂O₁₀
Molecular Weight:740.891
Hs Code.:

Synonyms:allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

There total 4 articles about allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1603826-95-4
allyl (2-O-benzoyl-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 1603826-96-5
allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With methanol; sodium methylate; at 20 - 60 ℃; for 19h; Inert atmosphere;

Reference yield:

: 1603826-94-3
2-O-benzoyl-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1603826-96-5
allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 0.33 h / -40 °C

2.1: sodium methylate; methanol / 19 h / 20 - 60 °C / Inert atmosphere

With methanol; sodium methylate; In toluene;

Reference yield:

: C₂₈H₃₀O₇

: 1603826-96-5
allyl (4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,2-dichloro-ethane / 0.5 h / 20 °C / Inert atmosphere

2.1: toluene / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 0.33 h / -40 °C

3.1: sodium methylate; methanol / 19 h / 20 - 60 °C / Inert atmosphere

With methanol; sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dichloro-ethane; toluene;