Technology Process of C17H15N
There total 5 articles about C17H15N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C12H10F3NO3S; phenylboronic acid;
In
1,2-dimethoxyethane;
at 20 ℃;
for 0.166667h;
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 1h;
DOI:10.1246/cl.131149
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 3 h / 150 °C
2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C
2.2: 1.5 h / 0 °C
3.1: 1,2-dimethoxyethane / 0.17 h / 20 °C
3.2: 1 h / 90 °C
With
potassium hexamethylsilazane;
In
tetrahydrofuran; 1,2-dimethoxyethane; toluene;
3.1: |Suzuki-Miyaura Coupling / 3.2: |Suzuki-Miyaura Coupling;
DOI:10.1246/cl.131149
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C
1.2: 1.5 h / -78 °C
1.3: 0.5 h / 70 °C
2.1: 3 h / 150 °C
3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C
3.2: 1.5 h / 0 °C
4.1: 1,2-dimethoxyethane / 0.17 h / 20 °C
4.2: 1 h / 90 °C
With
n-butyllithium; potassium hexamethylsilazane;
In
tetrahydrofuran; 1,2-dimethoxyethane; hexane; toluene;
4.1: |Suzuki-Miyaura Coupling / 4.2: |Suzuki-Miyaura Coupling;
DOI:10.1246/cl.131149