Technology Process of C27H32F3NO3S
There total 8 articles about C27H32F3NO3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
60percent sodium hydrate;
In
N,N-dimethyl-formamide;
at 10 - 30 ℃;
for 2h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; sodium carbonate / 5 h / Reflux
2: dmap / chloroform; toluene / 1 h / 75 °C / Inert atmosphere
3: 60percent sodium hydrate / N,N-dimethyl-formamide / 2 h / 10 - 30 °C / Cooling with ice
With
dmap; water; sodium carbonate;
In
chloroform; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: chloroform / 8 h / 0 °C
2.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux
2.2: 0.5 h / Reflux
3.1: water; sodium carbonate / 5 h / Reflux
4.1: dmap / chloroform; toluene / 1 h / 75 °C / Inert atmosphere
5.1: 60percent sodium hydrate / N,N-dimethyl-formamide / 2 h / 10 - 30 °C / Cooling with ice
With
dmap; water; sodium methylate; sodium carbonate;
In
tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide; toluene;
1.1: |Wittig Olefination;