3-[(4-Methylphenyl)sulfinyl]-2(5H)-furanone

Base Information

Chemical Name:3-[(4-Methylphenyl)sulfinyl]-2(5H)-furanone
CAS No.:108392-42-3
Molecular Formula:C₁₁H₁₀O₃S
Molecular Weight:222.265
Hs Code.:
DSSTox Substance ID:DTXSID701264078
Nikkaji Number:J895.752E

Synonyms:DTXSID701264078;108392-42-3;3-[(4-Methylphenyl)sulfinyl]-2(5H)-furanone

Suppliers and Price of 3-[(4-Methylphenyl)sulfinyl]-2(5H)-furanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[(4-Methylphenyl)sulfinyl]-2(5H)-furanone

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:222.03506535
Heavy Atom Count:15
Complexity:314

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)C2=CCOC2=O

Technology Process of 3-[(4-Methylphenyl)sulfinyl]-2(5H)-furanone

There total 2 articles about 3-[(4-Methylphenyl)sulfinyl]-2(5H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 85271-06-3
2-toluenethio-4-butenolide

: 108392-42-3
(+/-)-2-(p-tolylsulfinyl)-2-cyclopentenone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(01)90581-2

Reference yield:

: 108329-96-0
3,3-Bis-p-tolylsulfanyl-dihydro-furan-2-one

: 108392-42-3
(+/-)-2-(p-tolylsulfinyl)-2-cyclopentenone

Guidance literature:: Multi-step reaction with 2 steps

1: 89.1 percent / m-chloroperbenzoic acid / CHCl₃ / 0.17 h / 0 °C

2: 93.5 percent / m-chloroperbenzoic acid / CHCl₃ / 0.17 h / 0 °C

With 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1016/S0040-4020(01)90581-2

Reference yield:

: 108392-42-3
(+/-)-2-(p-tolylsulfinyl)-2-cyclopentenone

: 4-methyl-3-[(4-methylphenyl)sulfonyl]furan-2(5H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / m-CPBA / CH₂Cl₂ / 1 h / 20 °C

2: 43 percent / tetrahydrofuran / 48 h / 20 °C

3: 90 percent / toluene / 3 h / Heating

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo051574v