C₃₄H₃₃F₃INO₈

Base Information

Chemical Name:C₃₄H₃₃F₃INO₈
CAS No.:1392426-55-9
Molecular Formula:C₃₄H₃₃F₃INO₈
Molecular Weight:767.538
Hs Code.:

C<sub>34</sub>H<sub>33</sub>F<sub>3</sub>INO<sub>8</sub>

Synonyms:C₃₄H₃₃F₃INO₈

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Chemical Property of C₃₄H₃₃F₃INO₈

Chemical Property:

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Technology Process of C₃₄H₃₃F₃INO₈

There total 5 articles about C₃₄H₃₃F₃INO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1032989-92-6
C₂₄H₂₆INO₆

: 20445-33-4,39637-99-5
(R)-methoxytrifluoromethylphenylacetyl chloride

: 1392426-55-9
C₃₄H₃₃F₃INO₈

Guidance literature:: With pyridine; dmap; In dichloromethane; for 0.5h; Inert atmosphere;
DOI:10.1039/c2ob25100k

Reference yield:

: 40217-17-2,90719-32-7,120574-96-1,102029-44-7
(R)-4-(phenylmethyl)-2-oxazolidinone

: 1392426-55-9
C₃₄H₃₃F₃INO₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 - 0 °C / Inert atmosphere

2.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 2 h / Inert atmosphere

3.1: trityl tetrafluoroborate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / toluene / 1.5 h / -50 °C / Inert atmosphere

4.2: 1.5 h / -50 - -30 °C / Inert atmosphere

5.1: pyridine; dmap / dichloromethane / 0.5 h / Inert atmosphere

With pyridine; dmap; n-butyllithium; di-n-butylboryl trifluoromethanesulfonate; 20% palladium hydroxide on charcoal; hydrogen; trityl tetrafluoroborate; triethylamine; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; toluene; 4.1: Evans aldol coupling / 4.2: Evans aldol coupling;
DOI:10.1039/c2ob25100k

Reference yield:

: 137238-71-2
(4R)-3-[2-(Phenylmethoxy)acetyl]-4-(phenylmethyl)oxazolidin-2-one

: 1392426-55-9
C₃₄H₃₃F₃INO₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 2 h / Inert atmosphere

2.1: trityl tetrafluoroborate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / toluene / 1.5 h / -50 °C / Inert atmosphere

3.2: 1.5 h / -50 - -30 °C / Inert atmosphere

4.1: pyridine; dmap / dichloromethane / 0.5 h / Inert atmosphere

With pyridine; dmap; di-n-butylboryl trifluoromethanesulfonate; 20% palladium hydroxide on charcoal; hydrogen; trityl tetrafluoroborate; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; 3.1: Evans aldol coupling / 3.2: Evans aldol coupling;
DOI:10.1039/c2ob25100k