Rh₂(neopentyl isocyanide)6

Base Information

• Chemical Name: Rh₂(neopentyl isocyanide)6
• CAS No.: 85028-82-6
• Molecular Formula: C₃₆H₆₆N₆Rh₂
• Molecular Weight: 788.771

Synonyms:Rh₂(neopentyl isocyanide)6

Chemical Property of Rh₂(neopentyl isocyanide)6

Chemical Property:

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Technology Process of Rh₂(neopentyl isocyanide)6

There total 2 articles about Rh₂(neopentyl isocyanide)6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

(η5-pentamethylcyclopentadienyl)Rh-bis(neopentyl isocyanide) → neopentylaldimine + Rh2(neopentyl isocyanide)6 (85028-82-6) + 1,2,3,4-tetramethylfulvene (76089-59-3)

Guidance literature:

In benzene-d6; Irradiation (UV/VIS); A soln. of 2 equiv. Rh-complex in C6D6 is prepared in a quartz NMR tube and irradiated for 4 h with a 200 W high pressure Hg lamp.; removal of volatiles, detected by (1)H NMR;

Reference yield:

(η5-pentamethylcyclopentadienyl)Rh-bis(neopentyl isocyanide) + neopentylisonitrile (72443-18-6) → [Rh2(CNCH2C(CH3)3)6] (85028-82-6) + C6(2)H5CHNCH2C(CH3)3 (85028-84-8) + 1,2,3,4-tetramethylfulvene (76089-59-3) + C6D5CDNCH2C(CH3)3

Guidance literature:

In benzene-d6; Irradiation (UV/VIS); irradn. of Rh complex in C6D6 in presence of 2 equiv of CNCH2C(CH3)3; recrystd. from benzene/hexane;

DOI:10.1021/om00077a022

upstream raw materials:

neopentylisonitrile

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