1,3-phenylenediacetic acid dichloride

Base Information

• Chemical Name: 1,3-phenylenediacetic acid dichloride
• CAS No.: 52584-23-3
• Molecular Formula: C₁₀H₈Cl₂O₂
• Molecular Weight: 231.078

Synonyms:1,3-phenylenediacetic acid dichloride

Chemical Property of 1,3-phenylenediacetic acid dichloride

Chemical Property:

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Technology Process of 1,3-phenylenediacetic acid dichloride

There total 1 articles about 1,3-phenylenediacetic acid dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-bis(cyanomethyl)benzene (626-22-2) → 1,3-phenylenediacetic acid dichloride (52584-23-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / water / 1.5 h / Reflux

2: Vilsmeier reagent / dichloromethane / 0.17 h / 20 °C

With sulfuric acid; Vilsmeier reagent; In dichloromethane; water;

Reference yield: 100.0%

4-(1,3-dioxolan-2-yl)-N1-hydroxybenzenecarboximidamide (852691-00-0) + 1,3-phenylenediacetic acid dichloride (52584-23-3) → α,α'-bis{(4-[1,3]-dioxolan-2-yl)-O-carboxybenzamidoximo}-1,3-xylene (1003867-87-5)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1055/s-2007-990834

Reference yield: 92.0%

1,3-phenylenediacetic acid dichloride (52584-23-3) + toluene (108-88-3,15644-74-3,16713-13-6) → 2,2'-(1,3-phenylene)bis(1-(p-tolyl)ethanone)

Guidance literature:

1,3-phenylenediacetic acid dichloride; toluene; With aluminum (III) chloride; In dichloromethane; at 0 ℃; for 0.5h;

With hydrogenchloride;

DOI:10.1021/jacs.0c02101

upstream raw materials:

1,3-bis(cyanomethyl)benzene

Downstream raw materials:

C₂₆H₂₆N₄O₄

*,R^*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone>

{2-[3-(2-Oxo-2-ureido-ethyl)-phenyl]-acetyl}-urea

1-Methyl-3-(2-{3-[2-(3-methyl-ureido)-2-oxo-ethyl]-phenyl}-acetyl)-urea

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