4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane

Base Information

Chemical Name:4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane
CAS No.:88531-12-8
Molecular Formula:C₁₈H₂₂O₂S
Molecular Weight:302.437
Hs Code.:

Synonyms:4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane

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Chemical Property of 4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane

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Technology Process of 4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane

There total 3 articles about 4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 88531-11-7
3-bromomethyl-7-(p-tolylsulfonylmethyl)noradamantane

: 88531-12-8
4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 150 ℃; for 1h;

Reference yield:

: 770-14-9
3,7-dimethylenebicyclo[3.3.1]nonane

: 88531-12-8
4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 1 h / 90 °C

2: 92 percent / KOH / dimethylformamide / 1 h / 150 °C

With potassium hydroxide; In N,N-dimethyl-formamide;

Reference yield:

: 1950-69-2
toluene-p-sulfonyl bromide

: 88531-12-8
4-(p-tolylsulfonyl)-3,6-dehydrohomoadamantane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 1 h / 90 °C

2: 92 percent / KOH / dimethylformamide / 1 h / 150 °C

With potassium hydroxide; In N,N-dimethyl-formamide;