N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol

Base Information

Chemical Name:N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol
CAS No.:914080-60-7
Molecular Formula:C₄₂H₄₅NO₅
Molecular Weight:643.823
Hs Code.:

Synonyms:N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol

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Chemical Property of N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol

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Technology Process of N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol

There total 5 articles about N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,3S,4S,5R,6S)-1-Benzyl-3,4,5-tris-benzyloxy-6-benzyloxymethyl-piperidine-2-carbaldehyde

: 914080-60-7
N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -35 ℃; for 0.666667h;
DOI:10.1021/jo060890m

Reference yield:

: 914080-48-1
(2S,3S,4S,5R,6S)-N-benzyl-6-benzyloxymethyl-2-(thiazol-2-yl)-3,4,5-tribenzyloxypiperidine

: 914080-60-7
N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeI / acetonitrile / 0.25 h / 110 °C / microwave irradiation

1.2: NaBH₄ / CH₂Cl₂; methanol / 0.67 h / 0 - 20 °C

1.3: HgCl₂ / acetonitrile; H₂O; CH₂Cl₂

2.1: 52 mg / NaBH₄ / CH₂Cl₂; methanol / 0.67 h / -35 °C

With sodium tetrahydroborate; methyl iodide; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo060890m

Reference yield:

: 916585-87-0
(2R,3R,4R,5S,6S)-6-Benzylamino-1,3,4,5-tetrakis-benzyloxy-6-thiazol-2-yl-hexan-2-ol

: 914080-60-7
N-benzyl-2,6-dideoxy-2,6-imino-3,4,5,7-tetra-O-benzyl-L-glycero-D-idoheptitol

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N; TMEDA; MsCl / toluene / 1 h / 0 °C

1.2: 80 percent / Et₃N / acetonitrile / 0 - 85 °C

2.1: MeI / acetonitrile / 0.25 h / 110 °C / microwave irradiation

2.2: NaBH₄ / CH₂Cl₂; methanol / 0.67 h / 0 - 20 °C

2.3: HgCl₂ / acetonitrile; H₂O; CH₂Cl₂

3.1: 52 mg / NaBH₄ / CH₂Cl₂; methanol / 0.67 h / -35 °C

With sodium tetrahydroborate; N,N,N,N,-tetramethylethylenediamine; methanesulfonyl chloride; triethylamine; methyl iodide; In methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1021/jo060890m