Technology Process of 6,6'-di-O-(2-aminophenyl)-1',2,3,3',4,4'-hexa-O-methylsucroses
There total 5 articles about 6,6'-di-O-(2-aminophenyl)-1',2,3,3',4,4'-hexa-O-methylsucroses which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol; ethyl acetate;
at 20 ℃;
for 12h;
DOI:10.1021/ol301993d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ammonia; sodium / tetrahydrofuran / 2.33 h / -78 °C
2: triethylamine / dichloromethane / 1 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 24 h / 100 °C
4: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 12 h / 20 °C
With
palladium 10% on activated carbon; ammonia; hydrogen; sodium; potassium carbonate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol301993d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C
2: triethylamine / dichloromethane / 1 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 24 h / 100 °C
4: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 12 h / 20 °C
With
palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol301993d
