benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate

Base Information

Chemical Name:benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate
CAS No.:1091605-51-4
Molecular Formula:C₂₄H₂₇NO₆
Molecular Weight:425.481
Hs Code.:

Synonyms:benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate

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Chemical Property of benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate

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Technology Process of benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate

There total 1 articles about benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1091605-50-3
(2R,3S)-3-hydroxy-2-(2-oxopropyl)piperidine-1-carboxylic acid benzyl ester

: 501-53-1,94274-21-2
benzyl chloroformate

: 1091605-51-4
benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 3h; optical yield given as %ee;
DOI:10.1055/s-2008-1067271

Reference yield: 48.6%

: 1091605-51-4
benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate

: 6,8-dimethylpyrimido[5,4-b]pyridazin-4(3H )-one

: benzyl (2R,3S)-3-{[(benzyloxy)carbonyl]oxy}-2-[3-(6,8-dimethyl-4-oxopyrido[3,2-d]pyrimidin-3(4H)-yl)-2-oxopropyl]piperidine-1-carboxylate

Guidance literature:: benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate; With trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h;

With N-Bromosuccinimide; In dichloromethane; for 1h;

6,8-dimethylpyrimido[5,4-b]pyridazin-4(3H )-one; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 1091605-51-4
benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate

: C₂₄H₂₆BrNO₆

Guidance literature:: benzyl (2R,3S)-3-(((benzyloxy)carbonyl)oxy)-2-(2-oxopropyl)piperidine-1-carboxylate; With trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h;

With N-Bromosuccinimide; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1055/s-2008-1067271