methyl(phenyl)carbamoyl azide

Base Information

Chemical Name:methyl(phenyl)carbamoyl azide
CAS No.:859084-55-2
Molecular Formula:C₈H₈N₄O
Molecular Weight:176.178
Hs Code.:

Synonyms:methyl(phenyl)carbamoyl azide

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Chemical Property of methyl(phenyl)carbamoyl azide

Chemical Property:

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Technology Process of methyl(phenyl)carbamoyl azide

There total 3 articles about methyl(phenyl)carbamoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4285-42-1
N-phenyl-N-methylcarbamoyl chloride

: 859084-55-2
methyl(phenyl)carbamoyl azide

Guidance literature:: With sodium azide; ethanol;

Reference yield:

: 100-61-8
N-methylaniline

: 859084-55-2
methyl(phenyl)carbamoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: sodium azide / acetone / 12 h / 20 °C

With pyridine; sodium azide; In dichloromethane; acetone;
DOI:10.1021/acs.joc.0c00659

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 859084-55-2
methyl(phenyl)carbamoyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine; caesium carbonate / o-xylene / 12 h / 160 °C / Inert atmosphere

2: pyridine / dichloromethane / 0 - 20 °C

3: sodium azide / acetone / 12 h / 20 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; caesium carbonate; triphenylphosphine; In dichloromethane; o-xylene; acetone;
DOI:10.1021/acs.joc.0c00659