C₄₃H₅₀Br₂O₃S

Base Information

Chemical Name:C₄₃H₅₀Br₂O₃S
CAS No.:1542211-38-0
Molecular Formula:C₄₃H₅₀Br₂O₃S
Molecular Weight:806.742
Hs Code.:

C<sub>43</sub>H<sub>50</sub>Br<sub>2</sub>O<sub>3</sub>S

Synonyms:C₄₃H₅₀Br₂O₃S

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Chemical Property of C₄₃H₅₀Br₂O₃S

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Technology Process of C₄₃H₅₀Br₂O₃S

There total 6 articles about C₄₃H₅₀Br₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1542211-37-9
(2,6-diethynyl-4-(hexadecyloxy)benzyl)(ethyl)sulfane

: 188813-09-4
3-bromo-5-iodo-benzaldehyde

: 1542211-38-0
C₄₃H₅₀Br₂O₃S

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ja412606t

Reference yield:

: 1542211-35-7
C₃₃H₅₅BrOSi₂

: 1542211-38-0
C₄₃H₅₀Br₂O₃S

Guidance literature:: Multi-step reaction with 3 steps

1: 18 h / 20 °C / Schlenk technique; Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

3: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; 3: |Sonogashira Cross-Coupling;
DOI:10.1021/ja412606t

Reference yield:

: 1542211-33-5
5-(hexadecyloxy)-1,3-diiodo-2-methylbenzene

: 1542211-38-0
C₄₃H₅₀Br₂O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine / 35 °C

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 20 h / Reflux; Schlenk technique; Inert atmosphere

3: 18 h / 20 °C / Schlenk technique; Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

5: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; tetrabutyl ammonium fluoride; diethylamine; triethylamine; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; 1: |Sonogashira Cross-Coupling / 5: |Sonogashira Cross-Coupling;
DOI:10.1021/ja412606t