phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside
CAS No.:917568-44-6
Molecular Formula:C₂₀H₁₄Cl₄INO₅S
Molecular Weight:649.117
Hs Code.:

Synonyms:phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 286018-83-5
phenyl 2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

: 917568-44-6
phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; triphenylphosphine; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h;
DOI:10.1021/ja065907x

Reference yield: 92.0%

: 917568-44-6
phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

: 917568-45-7
phenyl 2,6-dideoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 70 ℃; for 1h;
DOI:10.1021/ja065907x

Reference yield:

: 917568-44-6
phenyl 6-iodo-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

: 917568-60-6
phenyl [2-(trimethylsilyl)ethyl 3,4-di-O-benzyl-2-O-benzoyl-β-D-galactopyrosyluronate]-(1->4)-2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside S-oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 92 percent / 2,2'-azobis(2-methylpropionitrile); tributyltin hydride / toluene / 1 h / 70 °C

2.1: 4-allyl-1,2-dimethoxybenzene / CH₂Cl₂ / 1 h / 20 °C

2.2: 75 percent / triflic anhydride; 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 1 h / -78 - 0 °C

3.1: 70 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 2 h / -78 - 0 °C

With 2,2'-azobis(isobutyronitrile); 1,2-dimethoxy-4-(2-propenyl)benzene; tri-n-butyl-tin hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1021/ja065907x