Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane

Base Information

Chemical Name:Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane
CAS No.:85719-60-4
Molecular Formula:C₁₆H₂₆O₂Si
Molecular Weight:278.467
Hs Code.:

Synonyms:Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane

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Chemical Property of Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane

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Technology Process of Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane

There total 2 articles about Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 588-72-7,1340-14-3
[(E)-2-bromoethenyl]benzene

: 85719-58-0
(diisopropoxymethylsilyl)methylmagnesium chloride

: 85719-60-4
Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane

Guidance literature:: With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In tetrahydrofuran; at 50 - 60 ℃;
DOI:10.1021/jo00160a046

Reference yield:

: 2212-08-0
(chloromethyl)(diisopropoxy)methylsilane

: 85719-60-4
Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Mg, dibromoethane / tetrahydrofuran

2: 100 percent / NiCl₂(Ph₂P(CH₂)3Ph₂P) / tetrahydrofuran / 50 - 60 °C

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); 1,1-Dibromoethane; magnesium; In tetrahydrofuran;
DOI:10.1021/jo00160a046

Reference yield: 51.0%

: 85719-60-4
Diisopropoxy-methyl-((E)-3-phenyl-allyl)-silane

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

Guidance literature:: With potassium fluoride; dihydrogen peroxide; In N,N-dimethyl-formamide; for 40h; Ambient temperature;
DOI:10.1021/jo00160a046