benzyl (2R,R_S)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide

Base Information

• Chemical Name: benzyl (2R,R_S)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide
• CAS No.: 167111-32-2
• Molecular Formula: C₂₂H₂₅N₃O₃S
• Molecular Weight: 411.525

Synonyms:benzyl (2R,R_S)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide

Chemical Property of benzyl (2R,R_S)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide

Chemical Property:

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Technology Process of benzyl (2R,R_S)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide

There total 1 articles about benzyl (2R,R_S)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.3%

ethoxycarbonyl 2-<(2R,RS)-2-benzylsulfinamoyl-4-oxoazetidin-1-yl>-3-methylbut-2-enoate (157027-16-2) + benzylamine (100-46-9) → benzyl (2R,RS)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide (167111-32-2)

Guidance literature:

In dichloromethane; at 0 - 25 ℃; for 1h;

DOI:10.1016/0040-4020(95)98705-M

Reference yield: 65.0%

benzyl (2R,RS)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide (167111-32-2) → benzyl (2R)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfonamide

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1016/0040-4020(95)98705-M

Reference yield: 60.0%

benzyl (2R,RS)-1-(1-benzylcarbamoyl-2-methylprop-1-enyl)-4-oxoazetidine-2-sulfinamide (167111-32-2) → (5S,6R)-4-benzyl-2-isopropylidene-5-oxo-5-thia-1,4-diazabicyclo<4.2.0>octane-3,8-dione (157087-75-7)

Guidance literature:

With hydrogenchloride; In dichloromethane; for 0.5h;

DOI:10.1016/0040-4020(95)98705-M

upstream raw materials:

ethoxycarbonyl 2-<(2R,R_S)-2-benzylsulfinamoyl-4-oxoazetidin-1-yl>-3-methylbut-2-enoate

benzylamine

Downstream raw materials:

(5S,6R)-4-benzyl-2-isopropylidene-5-oxo-5-thia-1,4-diazabicyclo<4.2.0>octane-3,8-dione

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