1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

Base Information

Chemical Name:1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate
CAS No.:1254815-53-6
Molecular Formula:CF₃O₃S*C₂₃H₃₀N₃
Molecular Weight:497.582
Hs Code.:

Synonyms:1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

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Chemical Property of 1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

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Technology Process of 1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

There total 5 articles about 1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1254815-47-8
1-(2,6-diisopropylphenyl)-4-phenyl-1H-[1,2,3]triazole

: 67-63-0,8013-70-5
isopropyl alcohol

: 1254815-53-6
1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

Guidance literature:: trifluoromethylsulfonic anhydride; isopropyl alcohol; With pyridine; In dichloromethane; at -20 - 20 ℃; for 1h;

1-(2,6-diisopropylphenyl)-4-phenyl-1H-[1,2,3]triazole; In dichloromethane; at -20 - 20 ℃;

Reference yield: 42.0%

: 41029-44-1
isopropyl triflate

: 1254815-47-8
1-(2,6-diisopropylphenyl)-4-phenyl-1H-[1,2,3]triazole

: 1254815-53-6
1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at -20 - 20 ℃;
DOI:10.1002/anie.201001864

Reference yield:

: 1254815-50-3
1-(2,6-diisopropylphenyl)-3-methyl-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

: 1254815-53-6
1-(2,6-diisopropylphenyl)-3-(2-propyl)-4-phenyl-1H-1,2,3-triazolium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 12 h / 50 °C

2.1: pyridine / dichloromethane / 1 h / -20 - 20 °C

2.2: -20 - 20 °C

With pyridine; potassium tert-butylate; In tetrahydrofuran; dichloromethane;