Technology Process of C24H34O3Si
There total 5 articles about C24H34O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate;
In
dichloromethane;
at -20 ℃;
for 12h;
Molecular sieve;
DOI:10.1016/j.tetlet.2012.04.118
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1H-imidazole / dichloromethane / 0 - 20 °C
2: methanol; toluene-4-sulfonic acid / 0 - 20 °C
3: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C
4: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve
With
1H-imidazole; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; L-(+)-diisopropyl tartrate; nickel diacetate; toluene-4-sulfonic acid;
In
ethanol; dichloromethane; ethylene glycol;
4: Sharpless epoxidation;
DOI:10.1016/j.tetlet.2012.04.118
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol; toluene-4-sulfonic acid / 0 - 20 °C
2: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C
3: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve
With
titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; L-(+)-diisopropyl tartrate; nickel diacetate; toluene-4-sulfonic acid;
In
ethanol; dichloromethane; ethylene glycol;
3: Sharpless epoxidation;
DOI:10.1016/j.tetlet.2012.04.118
