2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide

Base Information

• Chemical Name: 2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide
• CAS No.: 128080-89-7
• Molecular Formula: C₁₅H₁₅BrOS
• Molecular Weight: 323.253
• Mol file: 128080-89-7.mol

Synonyms:2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide

Chemical Property of 2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide

There total 1 articles about 2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.7%

6-(4-Bromobenzoyl)-1,3,4-trimethyl-2H-thiopyranium tetrafluoroborate → 2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide (128080-89-7)

Guidance literature:

With triethylamine; In ethanol; for 4h; ice-cooling;

DOI:10.1039/b102806p

Reference yield: 25.0%

2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide (128080-89-7) → 6-(4-Bromobenzoyl)-2,3,4-trimethyl-2H-thiopyran (128097-34-7) + 2-(4-Bromobenzoyl)-4,4,5-trimethyl-2H-thiopyran (128080-96-6) + 2-(4-Bromobenzoyl)-2,4,5-trimethyl-2H-thiopyran (128080-93-3) + 2-(4-Bromobenzoyl)-3a,6a-dihydro-3,6,6a-trimethylthieno[3,2-b]furan

Guidance literature:

In benzene; for 1.7h; Further Variations:; Solvents; Time; Product distribution; Heating;

DOI:10.1039/b102806p

Reference yield: 25.0%

2-(4-Bromobenzoyl)-1,4,5-trimethyl-1-thiabenzen-1-ium-2-ide (128080-89-7) → 6-(4-Bromobenzoyl)-2,3,4-trimethyl-2H-thiopyran (128097-34-7) + 2-(4-Bromobenzoyl)-4,4,5-trimethyl-2H-thiopyran (128080-96-6) + 2-(4-Bromobenzoyl)-2,4,5-trimethyl-2H-thiopyran (128080-93-3)

Guidance literature:

In benzene; for 1.7h; Heating;

DOI:10.1016/S0040-4039(00)94348-X

Downstream raw materials:

6-(4-Bromobenzoyl)-2,3,4-trimethyl-2H-thiopyran

2-(4-Bromobenzoyl)-4,4,5-trimethyl-2H-thiopyran

2-(4-Bromobenzoyl)-2,4,5-trimethyl-2H-thiopyran

2-[1-(4-Bromobenzoyl)ethyl]-3,4-dimethylthiophene