C₃₀H₃₈O₁₀

Base Information

• Chemical Name: C₃₀H₃₈O₁₀
• CAS No.: 1449477-39-7
• Molecular Formula: C₃₀H₃₈O₁₀
• Molecular Weight: 558.626
• Mol file: 1449477-39-7.mol

Synonyms:C₃₀H₃₈O₁₀

Chemical Property of C₃₀H₃₈O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₈O₁₀

There total 8 articles about C₃₀H₃₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C44H50O10 (1449477-36-4) → C30H38O10 (1449477-39-7)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 3h;

DOI:10.1002/asia.201201168

Reference yield:

C30H48O7Si → C30H38O10 (1449477-39-7)

Guidance literature:

Multi-step reaction with 8 steps

1.1: hydrogen fluoride / acetonitrile; water / 0.25 h / 0 °C

2.1: AD-mix α; methanesulfonamide / water; tert-butyl alcohol / 168 h / 0 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 40 °C / Inert atmosphere

4.1: triphenylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.2: 0.42 h / 20 °C / Inert atmosphere; Sonication

5.1: triphenylphosphine; gold(III) chloride; silver trifluoromethanesulfonate / dichloromethane / 7 h / 20 - 50 °C / Inert atmosphere

6.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

7.1: L-Selectride / tetrahydrofuran / 4 h / -78 °C / Inert atmosphere

8.1: hydrogen; palladium on activated charcoal / methanol / 3 h / 20 °C

With gold(III) chloride; methanesulfonamide; AD-mix α; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen fluoride; hydrogen; silver trifluoromethanesulfonate; L-Selectride; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol; 2.1: |Sharpless Dihydroxylation;

DOI:10.1002/asia.201201168

Reference yield:

C24H36O9 (1449477-34-2) → C30H38O10 (1449477-39-7)

Guidance literature:

Multi-step reaction with 6 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 40 °C / Inert atmosphere

2.1: triphenylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 0.42 h / 20 °C / Inert atmosphere; Sonication

3.1: triphenylphosphine; gold(III) chloride; silver trifluoromethanesulfonate / dichloromethane / 7 h / 20 - 50 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: L-Selectride / tetrahydrofuran / 4 h / -78 °C / Inert atmosphere

6.1: hydrogen; palladium on activated charcoal / methanol / 3 h / 20 °C

With gold(III) chloride; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen; silver trifluoromethanesulfonate; L-Selectride; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1002/asia.201201168

upstream raw materials:

C₂₄H₃₆O₉

C₂₄H₃₄O₈

C₄₄H₅₀O₁₀

C₄₄H₄₈O₁₀

Downstream raw materials:

epigallocatechin

Refernces