Benzenebutanoic acid, -gamma--(acetyloxy)--ba--methyl-, (-ba-S,-gamma-R)- (9CI)

Base Information

Chemical Name:Benzenebutanoic acid, -gamma--(acetyloxy)--ba--methyl-, (-ba-S,-gamma-R)- (9CI)
CAS No.:853759-96-3
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:
Mol file:853759-96-3.mol

Synonyms:Benzenebutanoicacid,-gamma--(acetyloxy)--bta--methyl-,(-bta-S,-gamma-R)-(9CI);Benzenebutanoic acid, -gamma--(acetyloxy)--ba--methyl-, (-ba-S,-gamma-R)- (9CI)

Suppliers and Price of Benzenebutanoic acid, -gamma--(acetyloxy)--ba--methyl-, (-ba-S,-gamma-R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Benzenebutanoic acid, -gamma--(acetyloxy)--ba--methyl-, (-ba-S,-gamma-R)- (9CI)

Chemical Property:

PSA：63.60000
LogP:2.40160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenebutanoic acid, -gamma--(acetyloxy)--ba--methyl-, (-ba-S,-gamma-R)- (9CI)

There total 4 articles about Benzenebutanoic acid, -gamma--(acetyloxy)--ba--methyl-, (-ba-S,-gamma-R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 853759-94-1
(1R,2S)-1-acetoxy-3-(4-methoxyphenyl)-2-methyl-1-phenylpropane

: 853759-96-3
(3S,4R)-4-acetoxy-3-methyl-4-phenylbutyric acid

Guidance literature:: With ruthenium trichloride; periodic acid; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2005.03.017

Reference yield:

: 853760-11-9
(1R,2S)-3-(4-methoxyphenyl)-2-methyl-1-phenyl-1-propanol

: 853759-96-3
(3S,4R)-4-acetoxy-3-methyl-4-phenylbutyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 4-dimethylaminopyridine / pyridine / 0.5 h / 20 °C

2: RuCl₃*H₂O; H₅IO₆ / CCl₄; acetonitrile; H₂O / 2 h / 20 °C

With dmap; ruthenium trichloride; periodic acid; In pyridine; tetrachloromethane; water; acetonitrile;
DOI:10.1016/j.tetasy.2005.03.017

Reference yield:

: 627875-76-7
(1S,4R)-1-[(1R,2R,3R)-3-Hydroxy-1-(4-methoxy-phenyl)-2-methyl-3-phenyl-propylsulfanylmethyl]-7,7-dimethyl-bicyclo[2.2.1]heptan-2-one

: 853759-96-3
(3S,4R)-4-acetoxy-3-methyl-4-phenylbutyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: Raney Ni W-2; aq. sodium hypophosphite monohydrate / ethanol; acetate buffer / 0.5 h / 20 °C / pH 5.2

2: 100 percent / 4-dimethylaminopyridine / pyridine / 0.5 h / 20 °C

3: RuCl₃*H₂O; H₅IO₆ / CCl₄; acetonitrile; H₂O / 2 h / 20 °C

With dmap; ruthenium trichloride; sodium hypophosphite; Raney Ni W-2; periodic acid; In pyridine; tetrachloromethane; ethanol; acetate buffer; water; acetonitrile;
DOI:10.1016/j.tetasy.2005.03.017