4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluorononyl azide

Base Information

• Chemical Name: 4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluorononyl azide
• CAS No.: 852527-60-7
• Molecular Formula: C₉H₆F₁₃N₃
• Molecular Weight: 403.146
• Hs Code.: 2929909090
• European Community (EC) Number: 632-949-7
• DSSTox Substance ID: DTXSID60465994
• Wikidata: Q82292343
• Mol file: 852527-60-7.mol

Synonyms:4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluorononyl azide;852527-60-7;9-Azido-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorononane;DTXSID60465994;DQEDVGBNEFVPEU-UHFFFAOYSA-N;NS00019270;4,4,5,5,6,6,7,7,8,8,9,9,9-TRIDECAFLUORONONYL AZIDE, PURUM, >=97.0% H-NMR

Chemical Property of 4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluorononyl azide

Chemical Property:

• Refractive Index: n20/D1.342
• PSA: 49.75000
• LogP: 5.26846
• XLogP3: 6.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 15
• Rotatable Bond Count: 8
• Exact Mass: 403.0354133
• Heavy Atom Count: 25
• Complexity: 517

Purity/Quality:

98%,99%, ^*data from raw suppliers

4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluorononyl azide ≥97.0% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CC(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)CN=[N+]=[N-]

Technology Process of 4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluorononyl azide

There total 1 articles about 4,4,5,5,6,6,7,7,8,8,9,9,9-Tridecafluorononyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluoro-9-iodononane (89889-20-3) → 9-azido-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorononane (852527-60-7)

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 100 ℃; for 5h;

DOI:10.1016/j.jfluchem.2016.08.005

upstream raw materials:

1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluoro-9-iodononane