(3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione

Base Information

• Chemical Name: (3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione
• CAS No.: 113405-25-7
• Molecular Formula: C₂₆H₂₂N₂O₃
• Molecular Weight: 410.472

Synonyms:(3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione

Chemical Property of (3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione

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Technology Process of (3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione

There total 4 articles about (3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

N-phenyl-maleimide (941-69-5) + Trifluoro-methanesulfonate3-methyl-2,5-diphenyl-oxazol-3-ium; → (3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione (113405-25-7) + (3aS,4R,6R,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione (113405-25-7,113472-75-6)

Guidance literature:

With phenylsilane; cesium fluoride; In acetonitrile; for 2h; Ambient temperature;

DOI:10.1021/ja00218a038

Reference yield: 55.0%

N-phenyl-maleimide (941-69-5) + Trifluoro-methanesulfonate3-methyl-2,5-diphenyl-oxazol-3-ium; → (3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione (113405-25-7) + (3aS,4R,6R,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione (113405-25-7,113472-75-6)

Guidance literature:

With phenylsilane; cesium fluoride; In acetonitrile; for 2h; Ambient temperature;

DOI:10.1021/ja00218a038

Reference yield:

N-phenyl-maleimide (941-69-5) + trans-1-methyl-2-benzoyl-3-phenylaziridine (7570-81-2) → (3aS,4S,6R,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione (113472-75-6) + (3aS,4S,6S,6aR)-4-Benzoyl-5-methyl-2,6-diphenyl-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione (113405-25-7)

Guidance literature:

In benzene; at 75 ℃; for 2h; Title compound not separated from byproducts;

DOI:10.1021/jo00244a009

upstream raw materials:

N-phenyl-maleimide

trans-1-methyl-2-benzoyl-3-phenylaziridine

cis-1-methyl-2-benzoyl-3-phenylaziridine

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