Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester

Base Information

Chemical Name:Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester
CAS No.:1026622-93-4
Molecular Formula:C₂₅H₃₀N₂O₄
Molecular Weight:422.524
Hs Code.:

Synonyms:Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester

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Chemical Property of Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester

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Technology Process of Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester

There total 4 articles about Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1975-52-6
5-nitro-o-toluic acid

: 1026622-93-4
Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / CH₂Cl₂

2: 71 percent / Et₃N / CH₂Cl₂ / 5 h / Ambient temperature

3: H₂ / 5percent Pd/C / ethyl acetate / 24 h / 760 Torr / Ambient temperature

4: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With thionyl chloride; hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm960153q

Reference yield:

: 64688-68-2
2-methyl-5-nitrobenzoyl chloride

: 1026622-93-4
Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / Et₃N / CH₂Cl₂ / 5 h / Ambient temperature

2: H₂ / 5percent Pd/C / ethyl acetate / 24 h / 760 Torr / Ambient temperature

3: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm960153q

Reference yield:

: 180136-10-1
2-methyl-5-nitro-N-(4-acetoxyphenyl)benzamide

: 1026622-93-4
Acetic acid 4-[5-(3-cyclohexyl-propionylamino)-2-methyl-benzoylamino]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent Pd/C / ethyl acetate / 24 h / 760 Torr / Ambient temperature

2: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm960153q