3,5-Di(11-dodecinyl)veratrol

Base Information

Chemical Name:3,5-Di(11-dodecinyl)veratrol
CAS No.:78476-79-6
Molecular Formula:C₃₂H₅₀O₂
Molecular Weight:466.748
Hs Code.:

Synonyms:3,5-Di(11-dodecinyl)veratrol

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Chemical Property of 3,5-Di(11-dodecinyl)veratrol

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Technology Process of 3,5-Di(11-dodecinyl)veratrol

There total 7 articles about 3,5-Di(11-dodecinyl)veratrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55362-80-6
9-bromononan-1-ol

: 78476-79-6
3,5-Di(11-dodecinyl)veratrol

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / diethyl ether; HCl / 24 h / 10 - 15 °C

2: 77 percent / K₂CO₃ / acetonitrile / 48 h / Heating

3: BuLi / tetrahydrofuran; hexane / 2 h / Ambient temperature

4: H₂ / 10 percent Pd/C / tetrahydrofuran / 3 h

5: 82 percent / 2 N H₂SO₄ / ethanol / 8 h / Heating

6: 83 percent / PPh₃, CCl₄ / 2 h / 80 - 90 °C

7: 94 percent / BuLi / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / Ambient temperature

With tetrachloromethane; n-butyllithium; sulfuric acid; hydrogen; potassium carbonate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; hexane; acetonitrile;

Reference yield:

: 55695-90-4
2-(9-bromononyloxy)tetrahydropyran

: 78476-79-6
3,5-Di(11-dodecinyl)veratrol

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / K₂CO₃ / acetonitrile / 48 h / Heating

2: BuLi / tetrahydrofuran; hexane / 2 h / Ambient temperature

3: H₂ / 10 percent Pd/C / tetrahydrofuran / 3 h

4: 82 percent / 2 N H₂SO₄ / ethanol / 8 h / Heating

5: 83 percent / PPh₃, CCl₄ / 2 h / 80 - 90 °C

6: 94 percent / BuLi / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / Ambient temperature

With tetrachloromethane; n-butyllithium; sulfuric acid; hydrogen; potassium carbonate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; acetonitrile;

Reference yield:

: 3937-56-2
1,9-Nonanediol

: 78476-79-6
3,5-Di(11-dodecinyl)veratrol

Guidance literature:: Multi-step reaction with 8 steps

1: 80 percent / 48 percent HBr / 72 h / 60 °C

2: 82 percent / diethyl ether; HCl / 24 h / 10 - 15 °C

3: 77 percent / K₂CO₃ / acetonitrile / 48 h / Heating

4: BuLi / tetrahydrofuran; hexane / 2 h / Ambient temperature

5: H₂ / 10 percent Pd/C / tetrahydrofuran / 3 h

6: 82 percent / 2 N H₂SO₄ / ethanol / 8 h / Heating

7: 83 percent / PPh₃, CCl₄ / 2 h / 80 - 90 °C

8: 94 percent / BuLi / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / Ambient temperature

With tetrachloromethane; n-butyllithium; sulfuric acid; hydrogen bromide; hydrogen; potassium carbonate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; hexane; acetonitrile;