C₃₉H₃₇N₇O₅

Base Information

Chemical Name:C₃₉H₃₇N₇O₅
CAS No.:1312611-24-7
Molecular Formula:C₃₉H₃₇N₇O₅
Molecular Weight:683.767
Hs Code.:

C<sub>39</sub>H<sub>37</sub>N<sub>7</sub>O<sub>5</sub>

Synonyms:C₃₉H₃₇N₇O₅

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Chemical Property of C₃₉H₃₇N₇O₅

Chemical Property:

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Technology Process of C₃₉H₃₇N₇O₅

There total 13 articles about C₃₉H₃₇N₇O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 103-82-2
phenylacetic acid

: 1312611-83-8
C₃₁H₃₁N₇O₄

: 1312611-24-7
C₃₉H₃₇N₇O₅

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 5332-25-2
6-bromoquinoline

: 1312611-24-7
C₃₉H₃₇N₇O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C / Cooling with ice

2.1: chloro-trimethyl-silane; triethylamine / N,N-dimethyl-formamide / 100 °C

3.1: hydrogenchloride; water / 19 h / Reflux

4.1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 7 h / 100 °C

5.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

6.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C

6.2: 20 °C

7.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 8 h / 100 - 110 °C

8.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

9.1: hydrogenchloride / methanol / 2 h / 20 °C

10.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; water; potassium acetate; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 8.1: Suzuki Coupling;

Reference yield:

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 1312611-24-7
C₃₉H₃₇N₇O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 20 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: hydrogenchloride / methanol / 2 h / 20 °C

5.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With hydrogenchloride; oxalyl dichloride; sodium hydride; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 3.1: Suzuki Coupling;