3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol

Base Information

Chemical Name:3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol
CAS No.:1364510-22-4
Molecular Formula:C₁₆H₁₃F₃O₄
Molecular Weight:326.272
Hs Code.:

Synonyms:3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol

Chemical Property:

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Technology Process of 3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol

There total 3 articles about 3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1364510-22-4
3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol

Guidance literature:: With aluminum (III) chloride; trichlorophosphate; at 0 - 20 ℃; for 10h; Inert atmosphere;

Reference yield:

: C₃₀H₂₃F₃O₄

: 1364510-22-4
3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol

Guidance literature:: With palladium on activated charcoal; hydrogen; In tetrahydrofuran; at 20 ℃; for 16h; under 760.051 Torr;
DOI:10.1016/j.bmcl.2017.01.086

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 1364510-22-4
3-(4-trifluoromethylphenyl)propanoyl-phloroglucinol

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0 - 70 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

3: palladium on activated charcoal; hydrogen / tetrahydrofuran / 16 h / 20 °C / 760.05 Torr

With palladium on activated charcoal; hydrogen; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2017.01.086