α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride

Base Information

Chemical Name:α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride
CAS No.:137650-36-3
Molecular Formula:C₂₄H₃₂N₂O₃*ClH
Molecular Weight:432.991
Hs Code.:

Synonyms:α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride

Chemical Property:

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Technology Process of α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride

There total 4 articles about α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(S)-2-(4-Hydroxy-2,6-dimethyl-phenyl)-1-((R)-1-methyl-2-oxo-6-phenyl-hexylcarbamoyl)-ethyl]-carbamic acid benzyl ester

: 137650-36-3
α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; under 1034.3 Torr; Yield given;
DOI:10.1021/jm00080a005

Reference yield:

: 123715-02-6
H-Dmt

: 137650-36-3
α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / 12.5percent aq. NaOH / 16 h

2: 4-methylmorpholine / tetrahydrofuran / 0.75 h / -23 °C

3: 4-methylmorpholine / tetrahydrofuran / 1.5 h

4: H₂, HCl / 5percent Pd/C / 1034.3 Torr

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00080a005

Reference yield:

: 137764-59-1
2,6-dimethyl-N-<(phenylmethoxy)carbonyl>-L-tyrosine

: 137650-36-3
α-amino-4-hydroxy-2,6-dimethyl-N-<1(R)-methyl-2-oxo-6-phenylhexyl>benzenepropanamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methylmorpholine / tetrahydrofuran / 0.75 h / -23 °C

2: 4-methylmorpholine / tetrahydrofuran / 1.5 h

3: H₂, HCl / 5percent Pd/C / 1034.3 Torr

With 4-methyl-morpholine; hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00080a005