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C29H34N2O4

Base Information
  • Chemical Name:C29H34N2O4
  • CAS No.:1256250-76-6
  • Molecular Formula:C29H34N2O4
  • Molecular Weight:474.6
  • Hs Code.:
C<sub>29</sub>H<sub>34</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C29H34N2O4

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Chemical Property of C29H34N2O4
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Technology Process of C29H34N2O4

There total 15 articles about C29H34N2O4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C30H36N2O4; With sodium hydroxide; In tetrahydrofuran; methanol; at 18 - 50 ℃; for 18h;
With acetic acid; In tetrahydrofuran; methanol; at 18 - 25 ℃;
Guidance literature:
Multi-step reaction with 4 steps
1.1: potassium acetate / 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere
2.1: ammonium formate / palladium 10% on activated carbon / methanol / 0.5 h / Reflux
3.1: sodium hydrogencarbonate / bis(tri-t-butylphosphine)palladium(0) / ISOPROPYLAMIDE; water / 16 h / 130 °C / Inert atmosphere; Sealed tube
4.1: sodium hydroxide / tetrahydrofuran; methanol / 18 h / 18 - 50 °C
4.2: 18 - 25 °C
With ammonium formate; potassium acetate; sodium hydrogencarbonate; sodium hydroxide; 1,1'-bis-(diphenylphosphino)ferrocene; bis(tri-t-butylphosphine)palladium(0); palladium 10% on activated carbon; In tetrahydrofuran; methanol; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide;
Guidance literature:
Multi-step reaction with 4 steps
1.1: perchloric acid / 6 h / 0 - 5 °C / Sealed tube
1.2: pH 8 - 9
2.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 16 h / 110 °C / Inert atmosphere; Sealed tube
3.1: sodium hydrogencarbonate / bis(tri-t-butylphosphine)palladium(0) / ISOPROPYLAMIDE; water / 16 h / 130 °C / Inert atmosphere; Sealed tube
4.1: sodium hydroxide / tetrahydrofuran; methanol / 18 h / 18 - 50 °C
4.2: 18 - 25 °C
With perchloric acid; sodium hydrogencarbonate; sodium carbonate; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; bis(tri-t-butylphosphine)palladium(0); In tetrahydrofuran; methanol; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide;
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