Technology Process of C29H34N2O4
There total 15 articles about C29H34N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H36N2O4;
With
sodium hydroxide;
In
tetrahydrofuran; methanol;
at 18 - 50 ℃;
for 18h;
With
acetic acid;
In
tetrahydrofuran; methanol;
at 18 - 25 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium acetate / 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere
2.1: ammonium formate / palladium 10% on activated carbon / methanol / 0.5 h / Reflux
3.1: sodium hydrogencarbonate / bis(tri-t-butylphosphine)palladium(0) / ISOPROPYLAMIDE; water / 16 h / 130 °C / Inert atmosphere; Sealed tube
4.1: sodium hydroxide / tetrahydrofuran; methanol / 18 h / 18 - 50 °C
4.2: 18 - 25 °C
With
ammonium formate; potassium acetate; sodium hydrogencarbonate; sodium hydroxide;
1,1'-bis-(diphenylphosphino)ferrocene; bis(tri-t-butylphosphine)palladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: perchloric acid / 6 h / 0 - 5 °C / Sealed tube
1.2: pH 8 - 9
2.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 16 h / 110 °C / Inert atmosphere; Sealed tube
3.1: sodium hydrogencarbonate / bis(tri-t-butylphosphine)palladium(0) / ISOPROPYLAMIDE; water / 16 h / 130 °C / Inert atmosphere; Sealed tube
4.1: sodium hydroxide / tetrahydrofuran; methanol / 18 h / 18 - 50 °C
4.2: 18 - 25 °C
With
perchloric acid; sodium hydrogencarbonate; sodium carbonate; sodium hydroxide;
bis-triphenylphosphine-palladium(II) chloride; bis(tri-t-butylphosphine)palladium(0);
In
tetrahydrofuran; methanol; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide;