(2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

Base Information

Chemical Name:(2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate
CAS No.:1255203-12-3
Molecular Formula:C₁₆H₂₂ClNO₅
Molecular Weight:343.807
Hs Code.:

Synonyms:(2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

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Technology Process of (2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

There total 14 articles about (2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1255203-04-3
ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-oxopropanoate

: 1255203-12-3
(2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

Guidance literature:: With dichloro(benzene)ruthenium(II) dimer; formic acid/triethylamine complex 5:2; (1S,2S)-2-(benzylamino)-1,2-diphenylethanol; In isopropyl alcohol; at 20 ℃; for 168h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/chem.201103739

Reference yield:

: 1255203-04-3
ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-oxopropanoate

: 1255203-12-3
(2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

: (2R,3R)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

Guidance literature:: With dichloro(benzene)ruthenium(II) dimer; triethylammonium formate; (1S,2S)-2-(benzylamino)-1,2-diphenylethanol; In isopropyl alcohol; at 20 ℃; for 168h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol102323k

Reference yield:

: 1255203-04-3
ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-oxopropanoate

: 1255203-12-3
(2S,3S)-ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

: ethyl 2-(tert-butoxycarbonylamino)-3-(3-chlorophenyl)-3-hydroxypropanoate

Guidance literature:: With dichloro(benzene)ruthenium(II) dimer; sodium formate; tetra-(n-butyl)ammonium iodide; triethylamine; (1S,2S)-2-(benzylamino)-1,2-diphenylethanol; In dichloromethane; water; at 0 - 20 ℃; pH=7; optical yield given as %ee; enantioselective reaction; Sonication;
DOI:10.1002/chem.201103739