[(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone

Base Information

• Chemical Name: [(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone
• CAS No.: 1189742-31-1
• Molecular Formula: C₃₉H₄₉N₃O₁₁S₂
• Molecular Weight: 799.964

Synonyms:[(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone

Chemical Property of [(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone

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Technology Process of [(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone

There total 1 articles about [(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

(2S)-N-[4-(3-bromopropoxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal (343308-55-4) + 2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol → [(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone (1189742-31-1)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Reflux;

DOI:10.1016/j.ejmech.2010.05.047

Reference yield:

[(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrol-1-yl]-[5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)-2-nitrophenyl]methanone (1189742-31-1) → [2-amino-5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)phenyl]{(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl}methanone (1189742-44-6)

Guidance literature:

With tin(II) chloride dihdyrate; In methanol; Reflux;

upstream raw materials:

(2S)-N-[4-(3-bromopropoxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal

Downstream raw materials:

[2-amino-5-methoxy-4-(3-{2-methoxy-5-[3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-5-isoxazolyl]phenoxy}propoxy)phenyl]{(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl}methanone

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