α,α,α-dichlorofluoromethoxybenzene

Base Information

• Chemical Name: α,α,α-dichlorofluoromethoxybenzene
• CAS No.: 1544-69-0
• Molecular Formula: C₇H₅Cl₂FO
• Molecular Weight: 195.021
• Mol file: 1544-69-0.mol

Synonyms:α,α,α-dichlorofluoromethoxybenzene

Chemical Property of α,α,α-dichlorofluoromethoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α,α,α-dichlorofluoromethoxybenzene

There total 3 articles about α,α,α-dichlorofluoromethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.2%

1-trifluoromethoxybenzene (456-55-3) → (trichloromethoxy)benzene (34888-05-6) + α,α,α-dichlorofluoromethoxybenzene (1544-69-0)

Guidance literature:

With aluminium trichloride; In dichloromethane; at 0 - 10 ℃; for 0.5h;

DOI:10.1081/SCC-120002522

Reference yield:

(trichloromethoxy)benzene (34888-05-6) → α,α,α-dichlorofluoromethoxybenzene (1544-69-0)

Guidance literature:

With triethylamine tris(hydrogen fluoride); at 50 ℃; for 25h;

DOI:10.1016/j.jfluchem.2005.10.006

Reference yield:

phenyl fluorothionoformate (1544-81-6) → α,α,α-dichlorofluoromethoxybenzene (1544-69-0)

Guidance literature:

With chlorine;

upstream raw materials:

phenyl fluorothionoformate

1-trifluoromethoxybenzene

(trichloromethoxy)benzene